HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrahydrofuran → HCID 69201252, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | 5-(benzyloxy)-2,3-dihydro-1H-inden-1-one | HCID 10752406 | — |
| Product | HCID 69201252 | HCID 69201252 | — |
Reaction Steps
5-Benzyloxyindanone (1.5 g, 6.29 mmol) was treated with NaH (60%, 377 mg) in THF (50 mL), and then Example 168A (1.59 g) was added. The reaction was stirred for 6 hours at room temperature. The precipitates were collected by filtration and dissolved in water, acidified with concentrated HCl, and the resulting precipitates were collected, washed with water and dried to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07320986B2 |
| Source dataset | uspto-grants-2008_01 |
| ORD ID | ord-a5e9da07e40643d0a40732639f5ba7d8 |
| Source note | uspto-grants-2008_01 |