HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → bis(4-methoxyphenyl)chloromethane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | p,p'-Dimethoxybenzhydryl alcohol | HCID 69768 | — |
| Product | bis(4-methoxyphenyl)chloromethane | HCID 10706646 | — |
Reaction Steps
Bis(4-methoxyphenyl)methanol (30 g) was treated with thionyl chloride (40 mL). The resulting mixture was refluxed for 2.5 hours and concentrated to give the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07320986B2 |
| Source dataset | uspto-grants-2008_01 |
| ORD ID | ord-6d59e8412476428fa6342a6116691eda |
| Source note | uspto-grants-2008_01 |