HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 69248711, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 58585365 | HCID 58585365 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 69248711 | HCID 69248711 | — |
Reaction Steps
0.2 ml of water and 2.2 ml of trifluoroacetic acid are added dropwise to a solution of 568 mg (0.889 mmol) of the compound from Example 2 in 4.5 ml of dichloromethane at room temperature. After 45 min, the reaction mixture is concentrated and thoroughly dried under high vacuum.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07320977B2 |
| Source dataset | uspto-grants-2008_01 |
| ORD ID | ord-714a3ff9a210468eb6eafaee2abc97fb |
| Source note | uspto-grants-2008_01 |