HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridinium chloride → 3-[2-(3,5-Dihydroxy-4-i-propylphenyl)ethenyl]benzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridinium chloride | HCID 10176127 | — |
| Reactant | 3-[2-(3,5-Dimethoxy-4-i-propylphenyl)ethenyl]benzoic acid | HCID 69099977 | — |
| Product | 3-[2-(3,5-Dihydroxy-4-i-propylphenyl)ethenyl]benzoic acid | HCID 66842749 | 86% |
Reaction Steps
This material was prepared from 3-[2-(3,5-dimethoxy-4-i-propylphenyl)ethenyl]benzoic acid 2B and pyridine hydrochloride in 86% yield in the same way as described in example 3. 1HNMR (DMSO-d6, ppm): δ 1.22 (d, J=7.0 Hz, 6H), 6.48 (s, 2H), 7.03 (d, J=17 Hz, 1H), 7.12 (d, J=17 Hz, 1H), 7.46 (t, J=7.5 Hz, 1H), 7.7-7.9 (m, 2H), 8.06 (s, 1H), 9.12 (s, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07321050B2 |
| Source dataset | uspto-grants-2008_01 |
| ORD ID | ord-147ced80c6184905a5df4294c21c25db |
| Source note | uspto-grants-2008_01 |