Iodoethane → 9-Ethoxymethyl-9-hydroxymethyl-fluorene

HRID 2252522Notes

Reaction equation

HRID 2252522 reaction equation
[OH:1][CH2:2][C:3]1([CH2:16][OH:17])[C:15]2[CH:14]=[CH:13][CH:12]=[CH:11][C:10]=2[C:9]2[C:4]1=[CH:5][CH:6]=[CH:7][CH:8]=2.[CH2:18](I)[CH3:19]>>[CH2:18]([O:1][CH2:2][C:3]1([CH2:16][OH:17])[C:15]2[CH:14]=[CH:13][CH:12]=[CH:11][C:10]=2[C:9]2[C:4]1=[CH:5][CH:6]=[CH:7][CH:8]=2)[CH3:19]

Participants

3

Reactant 2

HCID 6340IodoethaneHCID 3450229H-Fluorene-9,9-dimethanol

Product 1

HCID 693046709-Ethoxymethyl-9-hydroxymethyl-fluoreneYield 51%

Procedure

The target product as white crystal was prepared from 9,9-bis(hydroxymethyl)fluorene and ethyl iodide through the same procedure as described above. Yield: 51%.

Sources & evidence

ORD record
ord-d078af7c622d4e208021a276f2f36a90
Source dataset
uspto-grants-2008_01
Patent number
US07323431B2

Reaction notes

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