HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide dimethyl acetal → 3-Dimethylamino-3'-methoxyacrylophenone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| Reactant | 2-Propen-1-one, 1-(3-methoxyphenyl)- | HCID 10261393 | — |
| Product | 3-Dimethylamino-3'-methoxyacrylophenone | HCID 42573796 | — |
Reaction Steps
A mixture of 25 g. of m-methoxyacrylophenone and 25 ml. of dimethylformamide dimethyl acetal is refluxed for 12 hours. Removal of any volatile material in vacuo gives a thick oil. Bulb to bulb distillation gives the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04236005 |
| Source dataset | uspto-grants-1980_11 |
| ORD ID | ord-4f2753646c974de5a00c17ffbb06b68f |
| Source note | uspto-grants-1980_11 |