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HRID225253

反应详情

EQUATION

反应方程式

HRID 225253 的结构方程式

REACTANTS

反应物

2
结构：COC(OC)N(C)C
HCID78373

Methanamine, 1,1-dimethoxy-N,N-dimethyl-

C5H13NO2

结构：C=CC(=O)c1cccc(OC)c1
HCID10261393

2-Propen-1-one, 1-(3-methoxyphenyl)-

C10H10O2

PRODUCTS

生成物

1
结构：COc1cccc(C(=O)C=CN(C)C)c1
HCID42573796

3-(Dimethylamino)-1-(3-methoxyphenyl)prop-2-en-1-one

C12H15NO2

PROCEDURE

实验过程

A mixture of 25 g. of m-methoxyacrylophenone and 25 ml. of dimethylformamide dimethyl acetal is refluxed for 12 hours. Removal of any volatile material in vacuo gives a thick oil. Bulb to bulb distillation gives the desired product.

WORKUP

后处理

  1. additionA mixture of 25 g
  2. customRemoval of any volatile material in vacuo
  3. customgives a thick oil
  4. distillationBulb to bulb distillation