HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 23329856, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | 3-Dimethylamino-3'-trifluoromethylacrylophenone | HCID 730024 | — |
| Reactant | HCID 12239848 | HCID 12239848 | — |
| Product | HCID 23329856 | HCID 23329856 | — |
Reaction Steps
A mixture of 0.01 mole of 3-dimethylamino-3'-(trifluoromethyl)acrylophenone, 50 ml. of glacial acetic acid and 0.01 mole of 4-amino-2-methyl-5-imidazolecarbonitrile is refluxed for 5 hours. The solvent is removed under reduced pressure and the residue worked up as for Example 29 to give the product of the example.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04236005 |
| Source dataset | uspto-grants-1980_11 |
| ORD ID | ord-b0c9e31365d34a8eb573c7aa79b9239c |
| Source note | uspto-grants-1980_11 |