HRID225269

反应详情

EQUATION

反应方程式

HRID 225269 的结构方程式

PROCEDURE

实验过程

A mixture of 4.86 g. of 3-dimethylamino-3'-(trifluoromethyl)acrylophenone, 50 ml. of glacial acetic and 2.66 g. of 3-aminopyrazole-4,5-dicarbonitrile is refluxed for 10 hours and the solvent removed under reduced pressure. The residue is reacted with trifluoroacetic anhydride to give the product of the example.

WORKUP

后处理

  1. additionA mixture of 4.86 g
  2. customthe solvent removed under reduced pressure
  3. customThe residue is reacted with trifluoroacetic anhydride
  4. customto give the product of the example