huagongshe.com
HRID225281

反应详情

EQUATION

反应方程式

HRID 225281 的结构方程式

REACTANTS

反应物

2
结构：CCc1ccc(C(C)=O)cc1
HCID13642

p-Ethylacetophenone

C10H12O

结构：COC(OC)N(C)C
HCID78373

Methanamine, 1,1-dimethoxy-N,N-dimethyl-

C5H13NO2

PRODUCTS

生成物

1
结构：CCc1ccc(C(=O)C=CN(C)C)cc1
HCID53833899

未命名化合物

PROCEDURE

实验过程

A mixture of 50 g. of 4'-ethylacetophenone and 50 ml. of dimethylformamide dimethylacetal is refluxed for 16 hours. Evaporation gave a thick oil which crystallized on the addition of hexane, m.p. 80°-81° C.

WORKUP

后处理

  1. additionA mixture of 50 g
  2. customEvaporation
  3. customgave a thick oil which
  4. customcrystallized on the addition of hexane, m.p. 80°-81° C.