反应详情

2-(Azidomethyl)-4-chloro-N-methylbenzamide (0.88 g, 3.94 mmol) was dissolved in ethanol (25 mL), degassed, treated with 10% Pd on carbon (80 mg), and put under one atmosphere of hydrogen. After one hour the reaction was filtered through Celite, and concentrated in vacuo to afford 2-(aminomethyl)-N-methylbenzamide as a white solid.

1. customdegassed
2. additiontreated with 10% Pd on carbon (80 mg)
3. filtrationAfter one hour the reaction was filtered through Celite
4. concentrationconcentrated in vacuo