HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(azidomethyl)-4-chloro-N-methylbenzamide → 2-(aminomethyl)-N-methylBenzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(azidomethyl)-4-chloro-N-methylbenzamide | HCID 86600179 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 2-(aminomethyl)-N-methylBenzamide | HCID 23221198 | — |
Reaction Steps
2-(Azidomethyl)-4-chloro-N-methylbenzamide (0.88 g, 3.94 mmol) was dissolved in ethanol (25 mL), degassed, treated with 10% Pd on carbon (80 mg), and put under one atmosphere of hydrogen. After one hour the reaction was filtered through Celite, and concentrated in vacuo to afford 2-(aminomethyl)-N-methylbenzamide as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07323460B2 |
| Source dataset | uspto-grants-2008_01 |
| ORD ID | ord-65161268a57943528c12f6cddeccd3e2 |
| Source note | uspto-grants-2008_01 |