HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Bicarbonate → HCID 23329759, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Reactant | (-)-alpha-Amino-3-(chloromethyl)-4-hydroxybenzeneacetic acid hydrochloride | HCID 70578051 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 23329759 | HCID 23329759 | — |
Reaction Steps
To a solution of (-)-α-amino-3-(chloromethyl)-4-hydroxybenzeneacetic acid hydrochloride in water is added saturated aqueous sodium bicarbonate until a pH of 7 is reached. The solution is stirred overnight and is then lyophilized to give a quantitative yield of the title compound, combined with 2 equivalents of sodium chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04236002 |
| Source dataset | uspto-grants-1980_11 |
| ORD ID | ord-8e308c7fbb1a4de08831010b2d9a69ec |
| Source note | uspto-grants-1980_11 |