HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl Acrylate → HCID 86588344, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl Acrylate | HCID 7294 | — |
| Reactant | HCID 12332256 | HCID 12332256 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 86588344 | HCID 86588344 | 74% |
Reaction Steps
Prepared from the Heck coupling of 4-(4-bromophenyl)-1,2-dihydro-naphthalene (2i, compound I, R3=H, X=Br, and n=1) and methyl acrylate in accordance with the general method described in Example IV (J. Chem. Soc. B, 1969, 638-643). Yield 74%; APcI m/z: 332 (M+H+CH3CN+, 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07323587B2 |
| Source dataset | uspto-grants-2008_01 |
| ORD ID | ord-a90cc08d5c2948bb82610e7c72e146ab |
| Source note | uspto-grants-2008_01 |