Methyl Acrylate → HCID 69781329, compound

HRID 2253490Notes

Reaction equation

HRID 2253490 reaction equation
[C:1]1([CH:7]2[CH2:13][CH2:12][CH2:11][C:10]3[CH:14]=[CH:15][CH:16]=[CH:17][C:9]=3[CH:8]2[C:18]2[CH:23]=[CH:22][C:21](OS(C(F)(F)F)(=O)=O)=[CH:20][CH:19]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[C:32]([O:36][CH3:37])(=[O:35])[CH:33]=[CH2:34]>CC#N>[CH3:37][O:36][C:32](=[O:35])[CH:33]=[CH:34][C:21]1[CH:20]=[CH:19][C:18]([CH:8]2[C:9]3[CH:17]=[CH:16][CH:15]=[CH:14][C:10]=3[CH2:11][CH2:12][CH2:13][CH:7]2[C:1]2[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=2)=[CH:23][CH:22]=1

Participants

4

Reactant 2

HCID 7294Methyl AcrylateHCID 23573353HCID 23573353, compound

Product 1

HCID 69781329HCID 69781329, compound

Reagents, catalysts & solvents 1

HCID 6342AcetonitrileSolvent

Procedure

Prepared by Heck coupling 8c and methyl acrylate in accordance with the general method described in Example IV. Yield (14%); APcI m/z: 424 (M+H+CH3CN+, 100%).

Workup

  1. customPrepared by Heck
  2. customYield (14%)

Sources & evidence

ORD record
ord-135ee2b4021a48beaa11b50764abb1db
Source dataset
uspto-grants-2008_01
Patent number
US07323587B2

Reaction notes

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