Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 4-Cyanopyridine | HCID 7506 | — |
| Reactant | 1,4-Dibromobutane | HCID 8056 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 19745599 | HCID 19745599 | 226.3% |
Reaction Steps
A mixture of 4-cyanopyridine (12.5 g; 0.12 mol) and 1,4-dibromobutane (13 g; 0.06 mol) in dimethylformamide (50 ml) was stirred at 60° C. for 24 hours, and yellow precipitate was collected by filtration and washed with acetine to give tetramethylenebis(4-cyanopyridinium)dibromide (28.8 g). m.p., 296°-300° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05232574 |
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| Source dataset | uspto-grants-1993_08 |
|---|
| ORD ID | ord-6db1963ae603448298bb4179606206a6 |
|---|
| Source note | uspto-grants-1993_08 |
|---|
