HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,3-Propanedithiol → HCID 15020331, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,3-Propanedithiol | HCID 8013 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 86745117 | HCID 86745117 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 15020331 | HCID 15020331 | 95.9% |
Reaction Steps
A solution of trans-5-cyano-1,1-dimethyl-3-azido-indan-2-ol (0.93 g), triethylamine (1.2 ml) and 1,3-propanedithiol (0.9 ml) in dry methanol (20 ml) was stirred at room temperature for 48 h. After filtration, the solution was evaporated in vacuo to give the title compound (0.79 g) as a gum.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05232938 |
| Source dataset | uspto-grants-1993_08 |
| ORD ID | ord-e7438cf54bfb409faae6fdff2c89c3a4 |
| Source note | uspto-grants-1993_08 |