4-Toluenesulfonyl chloride → HCID 15105342, compound

HRID 2253679Notes

Reaction equation

HRID 2253679 reaction equation
O[CH2:2][CH2:3][CH2:4][N:5]1[C:14](=[O:15])[N:8]2[CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][C:7]2=[N:6]1.C1(C)C=CC(S([Cl:25])(=O)=O)=CC=1>>[Cl:25][CH2:2][CH2:3][CH2:4][N:5]1[C:14](=[O:15])[N:8]2[CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][C:7]2=[N:6]1

Participants

3

Reactant 2

HCID 73974-Toluenesulfonyl chlorideHCID 19746030HCID 19746030, compound

Product 1

HCID 15105342HCID 15105342, compound

Procedure

In the manner described in Reference Example 10-3), 2-(3-hydroxypropyl)-2,5,6,7,8,9-hexahydro-3H-1,2,4-triazolo-[4,3-a]azepin-3-one was treated with p-toluenesulfonyl chloride to obtain the entitled compound as an oily substance.

Workup

  1. customto obtain the entitled compound as an oily substance

Sources & evidence

ORD record
ord-19b88946661b4f828d9eea541b3d9ba5
Source dataset
uspto-grants-1993_08
Patent number
US05232924

Reaction notes

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