Methanol → 29443-23-0

HRID 2253739Notes

Reaction equation

HRID 2253739 reaction equation
CO.[CH2:3]([Br:6])[CH:4]=[CH2:5].[CH2:7]([N:9]([CH2:12][CH3:13])[CH2:10][CH3:11])[CH3:8]>>[Br-:6].[CH2:3]([N+:9]([CH2:12][CH3:13])([CH2:10][CH3:11])[CH2:7][CH3:8])[CH:4]=[CH2:5]

Participants

4

Reactant 3

HCID 887MethanolHCID 7841Allyl bromide2×HCID 8471Triethylamine

Product 1

HCID 12237729443-23-0

Procedure

A mixture of 60 grams of methanol, 60.23 grams of triethylamine and 60.72 grams of allyl bromide was prepared. The mixture was stirred for 5 minutes before refluxing. The mixture was allowed to reflux for 30 minutes before 12.0 grams of allyl bromide was added.

Workup

  1. customwas prepared
  2. temperaturebefore refluxing
  3. additionwas added

Sources & evidence

ORD record
ord-d080ba563d944f479fd7e8f3ba1de800
Source dataset
uspto-grants-1993_08
Patent number
US05232964

Reaction notes

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