HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 67233482, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Hexane | HCID 8058 | — |
| Reactant | 3-(Trimethoxysilyl)propyl chloride | HCID 62449 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 67233482 | HCID 67233482 | — |
Reaction Steps
A mixture of 60.0 grams of methanol, 60.0 grams of chloropropyltrimethoxysilane and 15.26 grams of pyridine was prepared. The mixture was heated and allowed to reflux for 72 hours. The mixture was vacuum stripped at 80° C. and 29 inches of Hg, for one hour. Following hexane and isopropanol washes, a white salt formed. The salt was dissolved in 15 grams of isopropanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05232964 |
| Source dataset | uspto-grants-1993_08 |
| ORD ID | ord-177ffcb62f2448b18b6ff50ae6df7669 |
| Source note | uspto-grants-1993_08 |