Methanol → HCID 67233482, compound

HRID 2253741Notes

Reaction equation

HRID 2253741 reaction equation
CO.[Cl:3][CH2:4][CH2:5][CH2:6][Si:7]([O:12][CH3:13])([O:10][CH3:11])[O:8][CH3:9].[N:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1.CCCCCC>C(O)(C)C>[Cl-:3].[CH3:9][O:8][Si:7]([CH2:6][CH2:5][CH2:4][N+:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1)([O:12][CH3:13])[O:10][CH3:11]

Participants

6

Reactant 4

HCID 887MethanolHCID 1049PyridineHCID 8058HexaneHCID 624493-(Trimethoxysilyl)propyl chloride

Product 1

HCID 67233482HCID 67233482, compound

Reagents, catalysts & solvents 1

HCID 3776IsopropanolSolvent2×

Procedure

A mixture of 60.0 grams of methanol, 60.0 grams of chloropropyltrimethoxysilane and 15.26 grams of pyridine was prepared. The mixture was heated and allowed to reflux for 72 hours. The mixture was vacuum stripped at 80° C. and 29 inches of Hg, for one hour. Following hexane and isopropanol washes, a white salt formed. The salt was dissolved in 15 grams of isopropanol.

Workup

  1. customwas prepared
  2. temperatureThe mixture was heated
  3. temperatureto reflux for 72 hours
  4. customstripped at 80° C.

Sources & evidence

ORD record
ord-177ffcb62f2448b18b6ff50ae6df7669
Source dataset
uspto-grants-1993_08
Patent number
US05232964

Reaction notes

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