Methanol → HCID 21677047, compound

Participants

Reaction Steps

Reactants used in the general procedure were phenyl N-trimethylsilylbenzenesulfonimidate (0.02 mol, 6.10 g) and methanol (0.06 mol, 2.5 ml). Reaction temperature was 22°-25° C.; reaction time was 4 hours. Stripping temperature was less than 35° C.; product yield was 95%. The 1H NMR spectrum of the product (200 MHz, 25% in CDCl3, 1 drop CH3CN) exhibited maxima at the following shift values: 3.78 (s, 1H, broad, NH); 6.88-8.01 (m, 10H, SC6H5, OC6H5).

Provenance & Evidence