HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Toluenesulfonic acid → HCID 57752207, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Toluenesulfonic acid | HCID 6101 | — |
| Reactant | HCID 12426268 | HCID 12426268 | — |
| Reactant | [(2-Methylacryloyl)oxy]acetic acid | HCID 13060939 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 57752207 | HCID 57752207 | — |
Reaction Steps
Hydroxycarbonylmethyl methacrylate (30 g) and dihydroxyadamantane (16.8) were added into dichloromethane (500 ml), and p-toluenesulfonic acid (1 g) was added thereto. Then, the mixture was refluxed for 15 hours while removing water generated. After the reaction, conventional after-treatments were carried out to obtain oil (21.2 g), which was identified to be Monomer A described above.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07556908B2 |
| Source dataset | uspto-grants-2009_07 |
| ORD ID | ord-65df79f8fb1645f5a42c2fdef4c0b081 |
| Source note | uspto-grants-2009_07 |