HRID225395

反应详情

EQUATION

反应方程式

HRID 225395 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

Hydroxycarbonylmethyl methacrylate (30 g) and dihydroxyadamantane (16.8) were added into dichloromethane (500 ml), and p-toluenesulfonic acid (1 g) was added thereto. Then, the mixture was refluxed for 15 hours while removing water generated. After the reaction, conventional after-treatments were carried out to obtain oil (21.2 g), which was identified to be Monomer A described above.

WORKUP

后处理

  1. additionwas added
  2. temperatureThen, the mixture was refluxed for 15 hours
  3. customwhile removing water
  4. customAfter the reaction