HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acrylic Acid → Ethylacrylate acrylic acid acrylonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acrylic Acid | HCID 6581 | — |
| Reactant | Acrylonitrile | HCID 7855 | — |
| Reactant | 1-Dodecanethiol | HCID 8195 | — |
| Reactant | Ethyl Acrylate | HCID 8821 | — |
| Reactant | Lauryl peroxide | HCID 76169 | — |
| Reactant | Butyl perbenzoate | HCID 83282 | — |
| Solvent | O-Xylene | HCID 7237 | — |
| Product | Ethylacrylate acrylic acid acrylonitrile | HCID 168852 | — |
Reaction Steps
this polymer material was produced by adding to 320 g xylene at 100° C. the monomer solution and a catalyst solution over a period of 3 hours. The monomer solution contained 2.900 g ethyl acrylate, 76 g acrylonitrile, 76 g acrylic acid and 3 g laurylmercaptan. The catalyst solution contained 26 g laurylperoxide and 7 g butylperbenzoate in 273 g of xylene. The material was highly viscous with comonomer proportions of 95:2.5:2.5.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05234730 |
| Source dataset | uspto-grants-1993_08 |
| ORD ID | ord-f2708cfb6e784dccac171806c4940e6b |
| Source note | uspto-grants-1993_08 |