huagongshe.com
HRID2254181

反应详情

EQUATION

反应方程式

HRID 2254181 的结构方程式

REACTANTS

反应物

3
结构：O=C([O-])[O-].[K+].[K+]
HCID11430

Potassium Carbonate

CK2O3

结构：O=[N+]([O-])c1ccc2cc[nH]c2c1
HCID78502

6-Nitro-1H-indole

C8H6N2O2

结构：COc1cc(C#N)ccc1CBr
HCID14752995

4-(Bromomethyl)-3-methoxybenzonitrile

C9H8BrNO

PRODUCTS

生成物

1
结构：COc1cc(C#N)ccc1Cn1ccc2ccc([N+](=O)[O-])cc21
HCID14752996

未命名化合物

收率 78%

PROCEDURE

实验过程

6-Nitroindole as alkylated with 4-bromomethyl-3-methoxybenzonitrile in the presence of potassium carbonate using the general procedure described. in Ex 1(a) to give 1-(4-cyano-2-methoxybenzyl)-6-nitroindole (W) in 78% yield as a solid, m.p. 190.5°-191° C.