HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → Benzenesulfinamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | Benzenesulfinyl chloride | HCID 4190003 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | Benzenesulfinamide | HCID 11286519 | 17% |
Reaction Steps
Benzenesulphinamide was prepared by reacting benzenesulphinyl chloride with ammonia in ether initially at -78° C. and finally at ambient temperature and was isolated in 17% yield as a solid, m.p. 112°-115° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05234942 |
| Source dataset | uspto-grants-1993_08 |
| ORD ID | ord-7fde7ad63c354631961f5d5b81c9d6fb |
| Source note | uspto-grants-1993_08 |