HuagongsheHuagongshe Chemistry Print Report · For research reference only
Glycidol → HCID 19745105, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Glycidol | HCID 11164 | — |
| Reactant | HCID 19745126 | HCID 19745126 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 19745105 | HCID 19745105 | 44% |
Reaction Steps
To a solution of 10 g (0.045 mol) of 230113 (Example 9--Step 3) in 60 ml of ethanol, are added 3.34 g (0.045 mol) of glycidol and left under stirring overnight. After concentration, the product is obtained by chromatography (silica, eluent: CH2Cl2 :97, CH3OH:3); Yield=44%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05235063 |
| Source dataset | uspto-grants-1993_08 |
| ORD ID | ord-838ae78a9d4d42f09f49db21b3a67c6c |
| Source note | uspto-grants-1993_08 |