反应详情

温度

-80 °C

Into a multineck glass reactor equipped with: magnetic entrainment mechanical stirrer, reflux cooler, thermocouple, inner plunging pipes for introducing the reagents, and maintained at a temperature of -80° C., there were simultaneously fed-after having introduced 75 of FC 75-0.5 l of bis(fluoroxy)difluoromethane at a flowrate of 0.3 l/h diluted with N2 (0.5 l/h) and 5.0 g of tetrafluoroethylene (3.0 g/h).

1. customInto a multineck glass reactor equipped with: magnetic entrainment mechanical stirrer
2. temperaturereflux cooler
3. additionthermocouple, inner plunging pipes for introducing the reagents