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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 2254323생성일: 2026년 10월 26일

Tetrafluoroethylene → 2,2,4,4,5,5-Hexafluoro-1,3-dioxolane

https://huagongshe.com/reaction/2254323

반응식

참여 물질

역할이름HCID투입량
반응물TetrafluoroethyleneHCID 8301—
반응물Bis(fluoroxy)perfluoromethaneHCID 140054—
용매NitrogenHCID 947—
생성물2,2,4,4,5,5-Hexafluoro-1,3-dioxolaneHCID 23234846—

반응 조건

온도-80 °C

반응 단계

Into a multineck glass reactor equipped with: magnetic entrainment mechanical stirrer, reflux cooler, thermocouple, inner plunging pipes for introducing the reagents, and maintained at a temperature of -80° C., there were simultaneously fed-after having introduced 75 of FC 75-0.5 l of bis(fluoroxy)difluoromethane at a flowrate of 0.3 l/h diluted with N2 (0.5 l/h) and 5.0 g of tetrafluoroethylene (3.0 g/h).

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US05235074
출처 데이터셋uspto-grants-1993_08
ORD IDord-5df94ef843ed4b2a9e4a793e59a1edab
출처 메모uspto-grants-1993_08