HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Fluorobenzaldehyde → HCID 54475519, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Fluorobenzaldehyde | HCID 68023 | — |
| Reactant | (5-Carboxypentyl)triphenylphosphanium bromide | HCID 2779280 | — |
| Product | HCID 54475519 | HCID 54475519 | 85.4% |
Reaction Steps
5-Carboxypentyl-triphenylphosphonium bromide (20 g) and 4-fluorobenzaldehyde (6.5 g) were subjected to substantially the same reaction as in Reference Example 1. The reaction product was isolated by means of a silica gel chromatography to afford 7-(4-fluorophenyl)-6-heptenoic acid (8.3 g) as white crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05235091 |
| Source dataset | uspto-grants-1993_08 |
| ORD ID | ord-52eb4b38095a495dab6bb646c3b24d25 |
| Source note | uspto-grants-1993_08 |