HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Ethyl 2-(hydroxymethyl)hexanal → 2-Butyl-2-ethyl-1,3-propanediol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Ethyl 2-(hydroxymethyl)hexanal | HCID 12538467 | — |
| Catalyst | Nickel | HCID 935 | — |
| Product | 2-Butyl-2-ethyl-1,3-propanediol | HCID 61038 | — |
Reaction Steps
continuously feeding the organic phase of step (8) to a hydrogenation zone wherein the 2-ethyl-2-(hydroxymethyl)hexanal is contacted with a supported nickel hydrogenation catalyst at a total pressure of about 21 to 36 bars absolute and at a hydrogenation zone exit temperature of about 150° to 170° C. to produce 2-butyl-2-ethyl-1,3-propanediol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05235118 |
| Source dataset | uspto-grants-1993_08 |
| ORD ID | ord-bd8d90fd6d5f45d5b2c3730f4880a837 |
| Source note | uspto-grants-1993_08 |