Thionyl Chloride → HCID 10799500, compound

HRID 2254403Notes

Reaction equation

HRID 2254403 reaction equation
[CH2:1]([C:9]1[CH:10]=[C:11]([CH:14]=[CH:15][CH:16]=1)[CH2:12]O)[CH2:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1.S(Cl)([Cl:19])=O>C(Cl)(Cl)Cl>[CH2:1]([C:9]1[CH:10]=[C:11]([CH:14]=[CH:15][CH:16]=1)[CH2:12][Cl:19])[CH2:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1

Participants

4

Reactant 2

HCID 24386Thionyl ChlorideHCID 10488743Benzenemethanol, 3-(2-phenylethyl)-

Product 1

HCID 10799500HCID 10799500, compoundYield 99%

Reagents, catalysts & solvents 1

HCID 6212ChloroformSolvent

Procedure

The resulting alcohol (140 mg) was dissolved in 1 ml of chloroform, and 0.3 ml of thionyl chloride was added. The mixture was reacted at room temperature for 30 minutes. The reaction mixture was evaporated under reduced pressure to give 150 mg (yield 99%) of 3-phenethylbenzyl chloride as a pale yellow oil.

Workup

  1. customThe mixture was reacted at room temperature for 30 minutes
  2. customThe reaction mixture was evaporated under reduced pressure

Sources & evidence

ORD record
ord-e0d091f11e3940e6979b2fad10b58995
Source dataset
uspto-grants-1993_08
Patent number
US05234946

Reaction notes

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