HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 10799500, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | Benzenemethanol, 3-(2-phenylethyl)- | HCID 10488743 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 10799500 | HCID 10799500 | 99% |
Reaction Steps
The resulting alcohol (140 mg) was dissolved in 1 ml of chloroform, and 0.3 ml of thionyl chloride was added. The mixture was reacted at room temperature for 30 minutes. The reaction mixture was evaporated under reduced pressure to give 150 mg (yield 99%) of 3-phenethylbenzyl chloride as a pale yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05234946 |
| Source dataset | uspto-grants-1993_08 |
| ORD ID | ord-e0d091f11e3940e6979b2fad10b58995 |
| Source note | uspto-grants-1993_08 |