Thionyl Chloride → HCID 178478433, compound

Participants

Reaction Conditions

Reaction Steps

90 mg of the hydrochloride was dissolved in 3 ml of chloroform, and 0.5 ml of thionyl chloride was added. The mixture was heated at 50° C. for 20 hours. The reaction mixture was evaporated under reduced pressure. The residue was washed with ethyl acetate and filtered to give 60 mg (yield 82%) of the captioned compound as a colorless crystalline powder.

Provenance & Evidence