HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 4674816, compound → HCID 53710459, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 4674816 | HCID 4674816 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 53710459 | HCID 53710459 | 92.1% |
Reaction Steps
144 mg of the resulting aldehyde compound was reduced with 15.6 mg of lithium aluminium hydride in 4 ml of tetrahydrofuran, and then worked up in a customary manner to give 134 mg (yield 92%) of the captioned compound as a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05234946 |
| Source dataset | uspto-grants-1993_08 |
| ORD ID | ord-9c4b7abe3b1c458ca78c82ad890147e5 |
| Source note | uspto-grants-1993_08 |