HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54195694, compound → HCID 53911071, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54195694 | HCID 54195694 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 53911071 | HCID 53911071 | 82.5% |
Reaction Steps
30 mg of the 3-(2,5-dihydro-3-thienyl)benzyl alcohol obtained in Referential Example 35 was dissolved in 25 ml of ethanol, and in the presence of 50 mg of 10% palladium-carbon, catalytically reduced for 8 hours under a hydrogen pressure of 3.5 kg/cm2. The catalyst was separated by filtration, and the solvent was evaporated under reduced pressure to give 25 mg (yield 82%) of the captioned compound as a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05234946 |
| Source dataset | uspto-grants-1993_08 |
| ORD ID | ord-c315cc7e6c7948d09d7765812247f513 |
| Source note | uspto-grants-1993_08 |