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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2254472Generated: October 31, 2026

HCID 54195694, compound → HCID 53911071, compound

https://huagongshe.com/reaction/2254472

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 54195694HCID 54195694—
CatalystHCID 178418390HCID 178418390—
SolventEthanolHCID 702—
ProductHCID 53911071HCID 5391107182.5%

Reaction Steps

30 mg of the 3-(2,5-dihydro-3-thienyl)benzyl alcohol obtained in Referential Example 35 was dissolved in 25 ml of ethanol, and in the presence of 50 mg of 10% palladium-carbon, catalytically reduced for 8 hours under a hydrogen pressure of 3.5 kg/cm2. The catalyst was separated by filtration, and the solvent was evaporated under reduced pressure to give 25 mg (yield 82%) of the captioned compound as a colorless oil.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05234946
Source datasetuspto-grants-1993_08
ORD IDord-c315cc7e6c7948d09d7765812247f513
Source noteuspto-grants-1993_08