HuagongsheHuagongshe Chemistry Print Report · For research reference only
Imidazole → HCID 19742631, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Imidazole | HCID 795 | — |
| Reactant | Diisopropylethylamine | HCID 81531 | — |
| Reactant | 2-Chloro-1-methylpyridinium iodide | HCID 167069 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 19742631 | HCID 19742631 | — |
Reaction Steps
2-Chloro-1-methylpyridinium iodide (9.43 g), imidazole (2.45 g) and diisopropylethylamine (4.77 g) were added to acetonitrile (150 ml) and the mixture refluxed for 2 hours. The product was filtered off from the chilled solution and dried. Yield, 6 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05236822 |
| Source dataset | uspto-grants-1993_08 |
| ORD ID | ord-42a2a9a725b3494f985916698b7796bf |
| Source note | uspto-grants-1993_08 |