Imidazole → HCID 19742631, compound

HRID 2254520Notes

Reaction equation

HRID 2254520 reaction equation
[I-:1].Cl[C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][N+:4]=1[CH3:9].[NH:10]1[CH:14]=[CH:13][N:12]=[CH:11]1.C(N(C(C)C)CC)(C)C>C(#N)C>[I-:1].[N:10]1([C:3]2[CH:8]=[CH:7][CH:6]=[CH:5][N+:4]=2[CH3:9])[CH:14]=[CH:13][N:12]=[CH:11]1

Participants

5

Reactant 3

HCID 795ImidazoleHCID 81531DiisopropylethylamineHCID 1670692-Chloro-1-methylpyridinium iodide

Product 1

HCID 19742631HCID 19742631, compound

Reagents, catalysts & solvents 1

HCID 6342AcetonitrileSolvent

Procedure

2-Chloro-1-methylpyridinium iodide (9.43 g), imidazole (2.45 g) and diisopropylethylamine (4.77 g) were added to acetonitrile (150 ml) and the mixture refluxed for 2 hours. The product was filtered off from the chilled solution and dried. Yield, 6 g.

Workup

  1. temperaturethe mixture refluxed for 2 hours
  2. filtrationThe product was filtered off from the chilled solution
  3. customdried
  4. customYield

Sources & evidence

ORD record
ord-42a2a9a725b3494f985916698b7796bf
Source dataset
uspto-grants-1993_08
Patent number
US05236822

Reaction notes

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