HuagongsheHuagongshe Chemistry Print Report · For research reference only
Azane;hydrate → HCID 136010432, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Azane;hydrate | HCID 12896473 | — |
| Reactant | HCID 57753062 | HCID 57753062 | — |
| Solvent | Chloroform methanol | HCID 21584188 | — |
| Product | HCID 136010432 | HCID 136010432 | — |
Reaction Steps
28% ammonia water was added to a chloroform-MeOH solution of methyl 2-[(4-chloro-2,5-difluorobenzoyl)amino]nicotinate and the resultant was stirred all night at room temperature to give 2-(4-chloro-2,5-difluorophenyl)pyrido[2,3-d]pyrimidine-4(3H)-one.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07557112B2 |
| Source dataset | uspto-grants-2009_07 |
| ORD ID | ord-6d48da911c6440469ce466e08df9128f |
| Source note | uspto-grants-2009_07 |