HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetyl chloride → HCID 18964220, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 18964213 | HCID 18964213 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 18964220 | HCID 18964220 | — |
Reaction Steps
0.12 g of acetyl chloride is added to 0.4 g of N-[4-(4-benzyl-4-hydroxypiperidyl) -2-(3,4-dichlorophenyl)butyl]-2,4-dichlorobenzamide hydrochloride (Compound 7), obtained according to Example 1, dissolved in 10 ml of dichloromethane in the presence of two equivalents of triethylamine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05236921 |
| Source dataset | uspto-grants-1993_08 |
| ORD ID | ord-1f86b5af1bdd46da95d6e7f42d9acfe5 |
| Source note | uspto-grants-1993_08 |