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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 225476Generated: October 31, 2026

1-Chloroethyl chloroformate → HCID 86615853, compound

https://huagongshe.com/reaction/225476

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1-Chloroethyl chloroformateHCID 521305—
ReactantHCID 10730982HCID 10730982—
ProductHCID 86615853HCID 86615853—

Reaction Steps

A mixture of ethyl (2E)-(1-benzyl-3-methylpiperidine-4-ylidene)acetate, 1-chloroethyl chloroformate and 1,2-dicholoroethane was stirred for 30 minutes heated to reflux and concentrated under reduced pressure. The residue was dissolved in EtOH and stirred for 10 minutes heated to reflux to give ethyl (2E)-(3-methylpiperidine-4-ylidene)acetate.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07557112B2
Source datasetuspto-grants-2009_07
ORD IDord-15c348654bd0412f8dbf9bc983dfcf83
Source noteuspto-grants-2009_07