Dichloromethane → HCID 54422511, compound

HRID 2254836Notes

Reaction equation

HRID 2254836 reaction equation
[OH:1][N:2]=[C:3]([C:6]1[CH:11]=[CH:10][CH:9]=[CH:8][CH:7]=1)[C:4]#[N:5].[CH2:12]([O:16][C:17]1[C:18]2[C:23]([C:24]([O:35][CH2:36][CH2:37][CH2:38][CH3:39])=[C:25]3[C:30]=1[CH:29]=[C:28]([S:31](Cl)(=[O:33])=[O:32])[CH:27]=[CH:26]3)=[CH:22][CH:21]=[CH:20][CH:19]=2)[CH2:13][CH2:14][CH3:15].ClCCl>C(N(CC)CC)C>[CH2:12]([O:16][C:17]1[C:18]2[C:23]([C:24]([O:35][CH2:36][CH2:37][CH2:38][CH3:39])=[C:25]3[C:30]=1[CH:29]=[C:28]([S:31]([O:1][N:2]=[C:3]([C:6]1[CH:11]=[CH:10][CH:9]=[CH:8][CH:7]=1)[C:4]#[N:5])(=[O:32])=[O:33])[CH:27]=[CH:26]3)=[CH:22][CH:21]=[CH:20][CH:19]=2)[CH2:13][CH2:14][CH3:15]

Participants

5

Reactant 3

HCID 6344DichloromethaneHCID 699982-(Hydroxyimino)-2-phenylacetonitrileHCID 19743175HCID 19743175, compound

Product 1

HCID 54422511HCID 54422511, compound

Reagents, catalysts & solvents 1

HCID 8471TriethylamineSolvent

Procedure

A mixture of 0.50 g of 2-hydroxyimino-2-phenylacetonitrile, 1.43 g of 9,10-dibutoxyanthracene-2-sulfonyl chloride and 20 ml of dichloromethane was stirred on an ice bath, and 0.34 g of triethylamine was added.

Sources & evidence

ORD record
ord-71f248e8657f43f9b8ce88578a8e5bbe
Source dataset
uspto-grants-1993_08
Patent number
US05237059

Reaction notes

Loading…