Acetone → HCID 11829456, compound

HRID 2254926Notes

Reaction equation

HRID 2254926 reaction equation
[CH3:1][C:2]([CH3:4])=O.[C:5]([NH:9][NH2:10])([CH3:8])([CH3:7])[CH3:6].[OH-].[K+]>CCOCC>[C:5]([NH:9][N:10]=[C:2]([CH3:4])[CH3:1])([CH3:8])([CH3:7])[CH3:6]

Participants

5

Reactant 3

HCID 180AcetoneHCID 14797Potassium HydroxideHCID 81890tert-Butylhydrazine

Product 1

HCID 11829456HCID 11829456, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

To 6.6 g of acetone, cooled in an ice bath, is added 5.0 g of tert-butylhydrazine. The mixture is stirred and then allowed to stand for several minutes. Ether and potassium hydroxide pellets are then added to the mixture. The mixture is stirred, and then the ethereal layer is separated from the mixture. Distillation of the ethereal layer yields the product acetone tert-butylhydrazone b.p. 132°-134° C.

Workup

  1. waitto stand for several minutes
  2. stirringThe mixture is stirred
  3. customthe ethereal layer is separated from the mixture
  4. distillationDistillation of the ethereal layer

Sources & evidence

ORD record
ord-54090dd792e74a9c8a7828e6d338f1a4
Source dataset
uspto-grants-1993_08
Patent number
US05237099

Reaction notes

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