HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetone → HCID 11829456, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetone | HCID 180 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | tert-Butylhydrazine | HCID 81890 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 11829456 | HCID 11829456 | — |
Reaction Steps
To 6.6 g of acetone, cooled in an ice bath, is added 5.0 g of tert-butylhydrazine. The mixture is stirred and then allowed to stand for several minutes. Ether and potassium hydroxide pellets are then added to the mixture. The mixture is stirred, and then the ethereal layer is separated from the mixture. Distillation of the ethereal layer yields the product acetone tert-butylhydrazone b.p. 132°-134° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05237099 |
| Source dataset | uspto-grants-1993_08 |
| ORD ID | ord-54090dd792e74a9c8a7828e6d338f1a4 |
| Source note | uspto-grants-1993_08 |