HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,5-Pyridinedicarboxylic acid → HCID 14210555, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,5-Pyridinedicarboxylic acid | HCID 7493 | — |
| Reactant | (+-)-Methyl mandelate | HCID 78066 | — |
| Product | HCID 14210555 | HCID 14210555 | — |
Reaction Steps
Analogously to Example 1, 10 g of pyridine-2,5-dicarboxylic acid are converted into the acid chloride and this is reacted with 19.9 g of methyl (±)-mandelate. After extraction, working up is carried out by chromatography over silica gel with a mixture of toluene and ethyl acetate as the mobile phase.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05238948 |
| Source dataset | uspto-grants-1993_08 |
| ORD ID | ord-b209a4f0d1d64f799bd0058062354069 |
| Source note | uspto-grants-1993_08 |