HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Fluoronitrobenzene → HCID 12874832, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Fluoronitrobenzene | HCID 9590 | — |
| Reactant | 3-(Dimethylamino)-1-phenylpropan-1-ol | HCID 110665 | — |
| Product | HCID 12874832 | HCID 12874832 | 88.5% |
Reaction Steps
Following the procedure of Example 3, 17.9 g of 3-dimethylamino-1-phenyl-1-propanol and 14.1 g of 1-fluoro-4-nitrobenzene were reacted to provide 26.54 g of the subtitle intermediate as a red oil. Preparation of the oxalate salt of a small portion of the oil provided yellow crystals with a melting point of 155°-157° C. (with decomposition).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05238959 |
| Source dataset | uspto-grants-1993_08 |
| ORD ID | ord-96f7f12ce73e463cae938e5b26dcfd07 |
| Source note | uspto-grants-1993_08 |