HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoic acid, 2-amino-5-iodo- → HCID 135493457, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoic acid, 2-amino-5-iodo- | HCID 72911 | — |
| Reactant | HCID 178440202 | HCID 178440202 | — |
| Product | HCID 135493457 | HCID 135493457 | — |
Reaction Steps
Following the procedure described as in the preparation of 6-nitro-2-propylquinazolin-4(1H)-one above. 25 g of 5-iodoanthranilic acid was converted into the title compound. 1H-NMR (CDCl3, 200 MHz): δ1.02 (t, 3H, J=7.4 Hz), 1.81 (m, 2H), 2.63 (t, 2H, J=7.4 Hz), 7.40 (d, 1H, J=8.6 Hz), 8.07 (dd, 1H, J=2, 8.7 Hz).1H, J=8.6 Hz), 8.07 (dd, 1H, J=2, 8.7 Hz).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05238942 |
| Source dataset | uspto-grants-1993_08 |
| ORD ID | ord-8a11361b84f54f71a4cc7d15cfa60f4a |
| Source note | uspto-grants-1993_08 |