Dicyclohexylamine → HCID 19742193, compound

HRID 2255346Notes

Reaction equation

HRID 2255346 reaction equation
[CH2:1]([N:5]1[C:9]2([CH2:14][O:13][P:12](Cl)[O:11][CH2:10]2)[CH2:8][O:7][P:6]1Cl)[CH:2]([CH3:4])[CH3:3].[CH:17]1([NH:23][CH:24]2[CH2:29][CH2:28][CH2:27][CH2:26][CH2:25]2)[CH2:22][CH2:21][CH2:20][CH2:19][CH2:18]1.C([N:32]([CH2:35][CH3:36])[CH2:33][CH3:34])C>C1(C)C=CC=CC=1>[CH2:1]([N:5]1[C:9]2([CH2:14][O:13][P:12]([N:23]([CH:17]3[CH2:18][CH2:19][CH2:20][CH2:21][CH2:22]3)[CH:24]3[CH2:25][CH2:26][CH2:27][CH2:28][CH2:29]3)[O:11][CH2:10]2)[CH2:8][O:7][P:6]1[N:32]([CH:33]1[CH2:34][CH2:26][CH2:25][CH2:24][CH2:29]1)[CH:35]1[CH2:36][CH2:19][CH2:18][CH2:17][CH2:22]1)[CH:2]([CH3:4])[CH3:3]

Participants

5

Reactant 3

HCID 7582DicyclohexylamineHCID 8471TriethylamineHCID 19742171HCID 19742171, compound

Product 1

HCID 19742193HCID 19742193, compound

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

The procedure of Example 10 is repeated using 1-isobutyl-2,8-dichloro-3,7,9-trioxa-1-aza-2,8-diphosphaspiro[4.5]decane, dicyclohexylamine and triethylamine in toluene to afford the desired product.

Sources & evidence

ORD record
ord-de1f7624bcdd4294b151cfd922aace7c
Source dataset
uspto-grants-1993_08
Patent number
US05239103

Reaction notes

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