HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → HCID 19738056, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | 1-Chloromethyl-1H-1,2,4-triazole | HCID 3743882 | — |
| Reactant | HCID 19738050 | HCID 19738050 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 19738056 | HCID 19738056 | — |
Reaction Steps
This compound (1.2 g.) was prepared using the procedure described in Example 2b except using 1.0 g. (3.3 mmoles) of 2-(4-chlorophenyl)-5-(2,6-dimethyl-4-morpholinyl)valeronitrile, 0.38 g. (3.3 mmoles) of 1-(chloromethyl)-1,2,4-triazole, and 0.16 g. (3.6 mmoles) of sodium hydride in 35 ml. of DMF and was isolated as a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05240925 |
| Source dataset | uspto-grants-1993_08 |
| ORD ID | ord-5378a2322146465996f8d4a91253da0c |
| Source note | uspto-grants-1993_08 |